Fabricating Novel Geometries of GA-CH Aerogels Through Wax Infiltration and Leaching of Fused Quartz

General Atomics-Carbon Hydrogen (GA-CH) and General Atomics-Carbon Deuterium (GA-CD) aerogels have applications as inertial confinement fusion (ICF) targets at the National Ignition Facility, Omega Laser Facility, and Z Pulsed Power Facility. However, fusion experiments at these facilities require the fabrication of precise geometries of aerogels, achievable only by machining. Unfortunately, machining low-density (<50 mg/cm³) GA-CH aerogels is difficult, given their fragile structure. Higher-density GA-CH aerogels, although easier to machine, are left with a small nub after machining. This work investigates filling the GA-CH gel pores with wax to increase their machinability. The wax was added by exchanging the solvent of the GA-CH gel with melted wax. In addition, 1- to 2-mm spherical voids were created within the aerogels using fused quartz beads that were leached with hydrofluoric acid. Samples were characterized for contaminants, structural damage, dopant loss, and surface roughness using size measurements, scanning electron microscopy, Fourier transform infrared spectroscopy, micro-computed tomography imaging, and optical profilometry. Through advances in aerogel fabrication techniques, progress is made toward testing new ICF target designs.