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A Low Temperature Distillation System for Separating Mixtures of Protium, Deuterium, and Tritium Isotopes

Michael C. Embury, Reed A. Watkins, Richard Hinckley, Arthur H. Post, Jr.

Fusion Science and Technology / Volume 8 / Number 2P2 / September 1985 / Pages 2168-2174

Blanket and Process Engineering / Proceedings of the Second National Topical Meeting on Tritium Technology in Fission, Fusion and Isotopic Applications (Dayton, Ohio, April 30 to May 2, 1985) / dx.doi.org/10.13182/FST85-A24604

A low temperature (24 K) distillation system for separating mixtures of hydrogen isotopes has been designed, fabricated, and delivered for use as the main component of the Hydrogen Isotope Separation System (HISS) at Mound. The HISS will handle feed mixtures of all six isotopic species of hydrogen (H2, HD, HT, D2, DT, T2) and will enrich the tritium while producing a stackable raffinate. Arthur D. Little, Inc. (ADL) was the prime contractor for the distillation system. The design and fabrication techniques used for the HISS distillation system are similar to those used for previous stills which were also designed and built by ADL. The distillation system was tested with mixtures of protium and deuterium at the ADL shop. This system, as well as the feed, product, and raffinate handling systems are presently being installed at Mound where integrated testing is scheduled next calendar year.