Fusion Science and Technology / Volume 37 / Number 2 / March 2000 / Pages 157-182
Technical Paper / dx.doi.org/10.13182/FST00-A132
Articles are hosted by Taylor and Francis Online.
Novel compounds containing hydrogen in new hydride and polymeric states that demonstrate novel hydrogen chemistry have been isolated following the electrolysis of a K2CO3 electrolyte with the production of excess energy. Inorganic hydride clusters K[KH KHCO3]n+ and hydrogen polymer ions such as OH23+ and H16- were identified by time-of-flight secondary ion mass spectroscopy. The presence of compounds containing new states of hydrogen was confirmed by X-ray photoelectron spectroscopy, X-ray diffraction, Fourier transform infrared spectroscopy, Raman spectroscopy, and proton nuclear magnetic resonance spectroscopy.